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  1. 教員研究業績
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Development and Evaluation of HILIC-type Sorbents Modified with Hydrophilic Copolymers for Solid-phase Extraction

https://gifu-pu.repo.nii.ac.jp/records/14521
https://gifu-pu.repo.nii.ac.jp/records/14521
622f6a96-03d4-4a40-ac66-28454f69b286
Item type 研究室原著論文(1)
公開日 2022-03-06
タイトル
タイトル Development and Evaluation of HILIC-type Sorbents Modified with Hydrophilic Copolymers for Solid-phase Extraction
言語
言語 eng
資源タイプ
資源タイプ識別子 http://purl.org/coar/resource_type/c_6501
資源タイプ journal article
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アクセス権 metadata only access
アクセス権URI http://purl.org/coar/access_right/c_14cb
抄録
値 Hydrophilic interaction chromatography (HILIC) has attractive attention for the separation of water-soluble compounds via HPLC. There are, however, few studies on the pretreatment of the HILIC-type solid-phase extraction (SPE) due to the difficulty of obtaining the HILIC-type sorbent. Therefore, the development of HILIC-type sorbents for SPE is essential. In this study, four different hydrophilic copolymers, namely diallylamine–maleic acid copolymer (DAM), diallylamine–acrylamide copolymer (DAA), allylamine–maleic acid copolymer (MAM), and partly methylcarbonylated allylamine acetate copolymer (MAC), were immobilized on glycidyl methacrylate (GMA)-base resin, and their adsorptive properties were evaluated. The results of the physical and adsorptive properties indicated that a balance between the water content of the water-enriched layer on sorbent and the amount of hydrophilic copolymer immobilized on the GMA-base resin was vital for the adsorption in HILIC-type sorbent for SPE.
書誌情報 en : Analytical Sciences

巻 36, 号 10, p. 1185-1190, 発行日 2020
DOI
値 10.2116/analsci.20P084
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