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  1. 教員研究業績
  2. 薬品分析化学研究室
  3. 原著論文

Simple Pretreatment and HILIC Separation for LC-ESI-MS/MS Determination of Adenosine in Human Plasma

https://gifu-pu.repo.nii.ac.jp/records/14522
https://gifu-pu.repo.nii.ac.jp/records/14522
daae746a-30a6-4d23-b063-0cab77aeeb3c
Item type 研究室原著論文(1)
公開日 2022-03-06
タイトル
タイトル Simple Pretreatment and HILIC Separation for LC-ESI-MS/MS Determination of Adenosine in Human Plasma
言語
言語 eng
資源タイプ
資源タイプ識別子 http://purl.org/coar/resource_type/c_6501
資源タイプ journal article
アクセス権
アクセス権 metadata only access
アクセス権URI http://purl.org/coar/access_right/c_14cb
抄録
値 A simple pretreatment method and separation mode for the LC-ESI-MS/MS determination of adenosine in human plasma have been developed. Deproteinization by acetonitrile and ultrafiltration followed by chromatographic separation with a hydrophilic interaction chromatographic (HILIC) column give a highly sensitive MS/MS response without ionic suppression caused by the matrix compounds in human plasma. In addition, the presence of ammonium acetate in the mobile phase contributes to high sensitivity in MS/MS detection, facilitating the ionization of adenosine. This method seems to be amenable to the treatment of many samples in clinical practice.
書誌情報 en : Analytical Sciences

巻 31, 号 11, p. 1189-1192, 発行日 2015
DOI
値 10.2116/analsci.31.1189
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