{"_buckets": {"deposit": "db9059c2-6095-4bd1-aec3-41413b610448"}, "_deposit": {"created_by": 5, "id": "7507", "owners": [5], "pid": {"revision_id": 0, "type": "depid", "value": "7507"}, "status": "published"}, "_oai": {"id": "oai:gifu-pu.repo.nii.ac.jp:00007507", "sets": ["181"]}, "author_link": ["25301", "11600", "26886", "25298", "25303", "26883", "11602", "26884", "26885", "25302", "25299", "25300"], "item_1_alternative_title_5": {"attribute_name": "論文名よみ", "attribute_value_mlt": [{"subitem_alternative_title": "〓"}]}, "item_1_biblio_info_14": {"attribute_name": "書誌情報", "attribute_value_mlt": [{"bibliographicIssueDates": {"bibliographicIssueDate": "1985-08-01", "bibliographicIssueDateType": "Issued"}, "bibliographicPageEnd": "13", "bibliographicPageStart": "10", "bibliographicVolumeNumber": "34", "bibliographic_titles": [{"bibliographic_title": "岐阜藥科大學紀要"}, {"bibliographic_title": "The annual proceedings of Gifu College of Pharmacy", "bibliographic_titleLang": "en"}]}]}, "item_1_creator_6": {"attribute_name": "著者名(日)", "attribute_type": "creator", "attribute_value_mlt": [{"creatorNames": [{"creatorName": "宇野, 文二"}], "nameIdentifiers": [{"nameIdentifier": "11600", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "加納, 健司"}], "nameIdentifiers": [{"nameIdentifier": "25298", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "河合, 聡"}], "nameIdentifiers": [{"nameIdentifier": "25299", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "窪田, 種一"}], "nameIdentifiers": [{"nameIdentifier": "25300", "nameIdentifierScheme": "WEKO"}]}]}, "item_1_creator_7": {"attribute_name": "著者名よみ", "attribute_type": "creator", "attribute_value_mlt": [{"creatorNames": [{"creatorName": "ウノ, ブンジ"}], "nameIdentifiers": [{"nameIdentifier": "26883", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "カノウ, ケンジ"}], "nameIdentifiers": [{"nameIdentifier": "26884", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "カワイ, サトシ"}], "nameIdentifiers": [{"nameIdentifier": "26885", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "クボタ, タネカズ"}], "nameIdentifiers": [{"nameIdentifier": "26886", "nameIdentifierScheme": "WEKO"}]}]}, "item_1_creator_8": {"attribute_name": "著者名(英)", "attribute_type": "creator", "attribute_value_mlt": [{"creatorNames": [{"creatorName": "UNO, BUNJI", "creatorNameLang": "en"}], "nameIdentifiers": [{"nameIdentifier": "11602", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "KANO, KENJI", "creatorNameLang": "en"}], "nameIdentifiers": [{"nameIdentifier": "25301", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "KAWAI, SATOSHI", "creatorNameLang": "en"}], "nameIdentifiers": [{"nameIdentifier": "25302", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "KUBOTA, TANEKAZU", "creatorNameLang": "en"}], "nameIdentifiers": [{"nameIdentifier": "25303", "nameIdentifierScheme": "WEKO"}]}]}, "item_1_description_1": {"attribute_name": "ページ属性", "attribute_value_mlt": [{"subitem_description": "P(論文)", "subitem_description_type": "Other"}]}, "item_1_description_11": {"attribute_name": "抄録(日)", "attribute_value_mlt": [{"subitem_description": "ヨードチンキのヨウ素酸滴定による定量は分析化学の学生実習において, 良い実習テーマの1つである。第十改正日本薬局方に収載されている定量法ではその操作中に濃塩酸(約12規定)50mlと水20mlを別々に加えることになっている。しかし, 学生達の健康面からしても, 比較的大量の濃塩酸を使用することはあまり推奨できることではない。この報告では, この定量法操作を改善するために, ヨードチンキのヨウ素酸滴定の正確さに対する塩酸濃度の影響について研究した。その結果, 塩酸2～3規定程度の薄い溶液中でもこの定量的な反応は円滑に進行することがわかった。従って結果としてこの定量法では直接濃塩酸を使用する代わりに6規定の塩酸(70ml)を使用することが, その取扱い易さから考えてもこの定量法操作に適していると考えられる。", "subitem_description_type": "Other"}]}, "item_1_description_12": {"attribute_name": "抄録(英)", "attribute_value_mlt": [{"subitem_description": "Quantitative analysis of iodo tincture is accepted as one of the good examples for the student experiments in the course of analytical chemistry. The J. P. X. employs 50ml of the ca. 12 N HCI and 20 ml of water in the analytical procedure. Since the treatment of the concentrated HCI is not so recommended from the viewpoint of student health, in this report, the influence of hydrochloric acid concentrations upon the titration accuracy in iodatimetry of iodo tincture has been studied in order to improve this analytical procedure. The results have indicated that the quantitative reaction proceeds smoothly even in the solution containing 2-3 N HCl, so that, as a result, the use of 6 N hydrochloric acid (70ml) instead of ca. 12 N HCI is possible in the prescription of the above analysis for more easy handling of the hydrochloric acid.", "subitem_description_type": "Other"}]}, "item_1_source_id_13": {"attribute_name": "雑誌書誌ID", "attribute_value_mlt": [{"subitem_source_identifier": "AN00053514", "subitem_source_identifier_type": "NCID"}]}, "item_1_text_10": {"attribute_name": "著者所属(英)", "attribute_value_mlt": [{"subitem_text_language": "en", "subitem_text_value": "Department of Pharmaceutical Analyses Gifu Pharmaceutical University/Department of Pharmaceutical Analyses Gifu Pharmaceutical University/Department of Pharmaceutical Analyses Gifu Pharmaceutical University/Department of Pharmaceutical Analyses Gifu Pharmaceutical University"}]}, "item_1_text_9": {"attribute_name": "著者所属(日)", "attribute_value_mlt": [{"subitem_text_value": "岐阜薬科大学/岐阜薬科大学/岐阜薬科大学/岐阜薬科大学"}]}, "item_files": {"attribute_name": "ファイル情報", "attribute_type": "file", "attribute_value_mlt": [{"accessrole": "open_date", "date": [{"dateType": "Available", "dateValue": "1985-08-01"}], "displaytype": "detail", "download_preview_message": "", "file_order": 0, "filename": "KJ00000071749.pdf", "filesize": [{"value": "234.8 kB"}], "format": "application/pdf", "future_date_message": "", "is_thumbnail": false, "licensetype": "license_free", "mimetype": "application/pdf", "size": 234800.0, "url": {"label": "KJ00000071749", "url": "https://gifu-pu.repo.nii.ac.jp/record/7507/files/KJ00000071749.pdf"}, "version_id": "473e9abc-1750-459b-a811-c4101ae2631c"}]}, "item_language": {"attribute_name": "言語", "attribute_value_mlt": [{"subitem_language": "jpn"}]}, "item_resource_type": {"attribute_name": "資源タイプ", "attribute_value_mlt": [{"resourcetype": "departmental bulletin paper", "resourceuri": "http://purl.org/coar/resource_type/c_6501"}]}, "item_title": "\u003c資料\u003e分析化学の学生実習に関する考察(第3報) : ヨードチンキのヨウ素酸滴定", "item_titles": {"attribute_name": "タイトル", "attribute_value_mlt": [{"subitem_title": "\u003c資料\u003e分析化学の学生実習に関する考察(第3報) : ヨードチンキのヨウ素酸滴定"}, {"subitem_title": "Discussion on Experiments of Analytical Chemistry for Students.III. : Iodatimetry of Iodo Tincture", "subitem_title_language": "en"}]}, "item_type_id": "1", "owner": "5", "path": ["181"], "permalink_uri": "https://gifu-pu.repo.nii.ac.jp/records/7507", "pubdate": {"attribute_name": "公開日", "attribute_value": "1985-08-01"}, "publish_date": "1985-08-01", "publish_status": "0", "recid": "7507", "relation": {}, "relation_version_is_last": true, "title": ["\u003c資料\u003e分析化学の学生実習に関する考察(第3報) : ヨードチンキのヨウ素酸滴定"], "weko_shared_id": 5}