{"created":"2023-06-19T07:23:28.069563+00:00","id":8097,"links":{},"metadata":{"_buckets":{"deposit":"06c08134-bb54-4676-a7f0-314818b6e224"},"_deposit":{"created_by":5,"id":"8097","owners":[5],"pid":{"revision_id":0,"type":"depid","value":"8097"},"status":"published"},"_oai":{"id":"oai:gifu-pu.repo.nii.ac.jp:00008097","sets":["147:183"]},"author_link":["26270","21232","26272","26267","21231","21233","26268","26269","26271"],"item_1_alternative_title_5":{"attribute_name":"論文名よみ","attribute_value_mlt":[{"subitem_alternative_title":"〓"}]},"item_1_biblio_info_14":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"1987-06-30","bibliographicIssueDateType":"Issued"},"bibliographicPageEnd":"52","bibliographicPageStart":"49","bibliographicVolumeNumber":"36","bibliographic_titles":[{"bibliographic_title":"岐阜藥科大學紀要"},{"bibliographic_title":"The annual proceedings of Gifu College of Pharmacy","bibliographic_titleLang":"en"}]}]},"item_1_creator_6":{"attribute_name":"著者名(日)","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"高野, 正樹"}],"nameIdentifiers":[{"nameIdentifier":"26267","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"平光, 敦"}],"nameIdentifiers":[{"nameIdentifier":"26268","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"河合, 聡"}],"nameIdentifiers":[{"nameIdentifier":"21231","nameIdentifierScheme":"WEKO"}]}]},"item_1_creator_7":{"attribute_name":"著者名よみ","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"タカノ, マサキ"}],"nameIdentifiers":[{"nameIdentifier":"26269","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"ヒラミツ, アツシ"}],"nameIdentifiers":[{"nameIdentifier":"26270","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"カワイ, サトシ"}],"nameIdentifiers":[{"nameIdentifier":"21232","nameIdentifierScheme":"WEKO"}]}]},"item_1_creator_8":{"attribute_name":"著者名(英)","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"TAKANO, MASAKI","creatorNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"26271","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"HIRAMITSU, ATSUSHI","creatorNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"26272","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"KAWAI, SATOSHI","creatorNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"21233","nameIdentifierScheme":"WEKO"}]}]},"item_1_description_1":{"attribute_name":"ページ属性","attribute_value_mlt":[{"subitem_description":"P(論文)","subitem_description_type":"Other"}]},"item_1_description_11":{"attribute_name":"抄録(日)","attribute_value_mlt":[{"subitem_description":"ガスクロマトグラフィーによる製剤中テオフィリンの簡易定量法を確立した。製剤中テオフィリンを0.1N水酸化ナトリウム試液で抽出した液にカウンターイオンとして臭化テトラブチルアンモニウムを加えたのち, ヨウ化メチルと内部標準物質(ステアリン酸メチル)を含むジクロルメタンで抽出メチル化し, その一定量を濃縮することなくガスクロマトグラフに注入した。分離条件は3%SE-30,2.Om, 200℃, FIDである。","subitem_description_type":"Other"}]},"item_1_description_12":{"attribute_name":"抄録(英)","attribute_value_mlt":[{"subitem_description":"A simple method for the determination of theophylline in preparations by gas chromatography (GC) after extractive methylation is described. Theophylline in preparations is extracted with 0.1N sodium hydroxide by shaking. To a 2.5 ml aliquot of the sample solution obtained, a counter-ion (tetrabutylammonium bromide) solution is added and the mixture is extracted into methylene chloride containing methyl iodide and an internal standard (methyl stearate). Extraction and methylation of theophylline proceed simultaneously. An aliquot of the extract is injected without evaporation into GC. GC is carried out at 200℃ on a 2.0 m of glass column packed with 3% SE-30.","subitem_description_type":"Other"}]},"item_1_source_id_13":{"attribute_name":"雑誌書誌ID","attribute_value_mlt":[{"subitem_source_identifier":"AN00053514","subitem_source_identifier_type":"NCID"}]},"item_1_text_10":{"attribute_name":"著者所属(英)","attribute_value_mlt":[{"subitem_text_language":"en","subitem_text_value":"Kyowa Pharmaceutical CO., Ltd./Kyowa Pharmaceutical CO., Ltd./Department of Pharmacutical Analytical Chemistry, Gifu Pharmaceutical University"}]},"item_1_text_9":{"attribute_name":"著者所属(日)","attribute_value_mlt":[{"subitem_text_value":"協和薬品工業株式会社/協和薬品工業株式会社/岐阜薬科大学"}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"1987-06-30"}],"displaytype":"detail","filename":"KJ00000072023.pdf","filesize":[{"value":"217.2 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"url":"https://gifu-pu.repo.nii.ac.jp/record/8097/files/KJ00000072023.pdf"},"version_id":"3bb2c348-eaed-4974-bda9-02345934e1a6"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"jpn"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"departmental bulletin paper","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"<ノート>抽出メチル化による製剤中テオフィリンのガスクロマトグラフィー","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"<ノート>抽出メチル化による製剤中テオフィリンのガスクロマトグラフィー"},{"subitem_title":"<Note>Gas Chromatographic Determination of Teophylline in Preparations after Extractive Methylation","subitem_title_language":"en"}]},"item_type_id":"1","owner":"5","path":["183"],"pubdate":{"attribute_name":"公開日","attribute_value":"1987-06-30"},"publish_date":"1987-06-30","publish_status":"0","recid":"8097","relation_version_is_last":true,"title":["<ノート>抽出メチル化による製剤中テオフィリンのガスクロマトグラフィー"],"weko_creator_id":"5","weko_shared_id":5},"updated":"2023-06-19T08:07:07.956349+00:00"}