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Synthesis, Characterization, and Reactivity of an Ethynyl Benziodoxolone (EBX)–Acetonitrile Complex

https://gifu-pu.repo.nii.ac.jp/records/13445
https://gifu-pu.repo.nii.ac.jp/records/13445
8555e61e-5b95-4753-97a0-83aff0c77cf8
Item type 研究室原著論文(1)
公開日 2019-03-04
タイトル
タイトル Synthesis, Characterization, and Reactivity of an Ethynyl Benziodoxolone (EBX)–Acetonitrile Complex
言語 en
言語
言語 eng
資源タイプ
資源タイプ識別子 http://purl.org/coar/resource_type/c_6501
資源タイプ journal article
アクセス権
アクセス権 metadata only access
アクセス権URI http://purl.org/coar/access_right/c_14cb
抄録
値 The synthesis of a cryst. ethynyl-1,2-benziodoxol-3(1H)-one (EBX)-acetonitrile complex is described.  EBX has been widely used as an active species for a variety of reactions; however, its high instability has so far prevented its isolation.  The EBX-acetonitrile is self-assembled into a double-layered honeycomb structure through weak hypervalent iodine secondary interactions and hydrogen bonding.  The N-ethynylation of a variety of sulfonamides using the EBX-acetonitrile complex as a substrate under mild conditions is also described.
書誌情報 en : Organic Letters

巻 21, 号 4, p. 1098-1102, 発行日 2019-02-15
DOI
値 10.1021/acs.orglett.9b00005
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